Xiaoyong Lu - One-pot preparation of fluorinated a-aminoalkyl phosphonates under microwave irradiation and solvent-free condition

Document created by Xiaoyong Lu on Aug 22, 2014
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  Publication Details (including relevant citation   information):

  A facile one-pot method has been developed for the synthesis of   fluorine-containing agr-amino  phosphonates in good   yields by a three-component reaction of  fluorinated   aromatic aldehydes, anilines, and diethyl phosphate in the    presence of a silica-gel support under microwave irradiation   within  10 min.

  Abstract:

  A facile one-pot method has been developed for the synthesis of   fluorine-containing agr-amino  phosphonates in good   yields by a three-component reaction of  fluorinated   aromatic aldehydes, anilines, and diethyl phosphate in the    presence of a silica-gel support under microwave irradiation   within  10 min. All new compounds are fully characterized by   spectral methods  and elemental analysis.

  Address (URL): http://www.informaworld.com/smpp/content~db=all~content=a770967661

 

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