Nura Suleiman Gwaram - Chlorido(2-{1-[(2-morpholinoethyl)- imino]ethyl}phenolato-j3N,N00,O)- copper(II)

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  Publication Details (including relevant citation   information):

  Acta Cryst. (2011). E67, m57 [ doi:10.1107/S1600536810051160 ]

  Nurul Azimah Ikmal Hisham, Nura Suleiman Gwaram,
  Hamid Khaledi* and Hapipah Mohd Ali
  Department of Chemistry, University of Malaya, 50603 Kuala   Lumpur, Malaysia
  Correspondence e-mail: khaledi@siswa.um.edu.my
  Received 2 December 2010; accepted 6 December 2010
  Key indicators: single-crystal X-ray study; T = 100 K; mean (C–C)   = 0.006 A°
  ;
  R factor = 0.043; wR factor = 0.096; data-to-parameter ratio =   13.7.

  Abstract:

  In the title compound, [CuCl(C14H19N2O2)], the CuII ion is
  four-coordinated by one deprotonated N,N0,O-tridentate
  Schiff base and one chloride ion in a distorted square-planar
  geometry. In the crystal, adjacent molecules are linked via   C—
  H Cl and C—H O interactions, forming infinite layers
  parallel to the (100) plane. The structure was determined   from
  a non-merohedrally twined crystal [twin ratio 0.777 (3):
  0.223 (3)].

  Key indicators: single-crystal X-ray study; T = 100 K; mean (C–C)   = 0.006 A°
  ;
  R factor = 0.043; wR factor = 0.096; data-to-parameter ratio =   13.7.

  Address (URL): http://journals.iucr.org/e/

 

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