Jason Schaff - An HPLC-HR-MS-MS Method for Identification of Anticoagulant Rodenticides in Blood

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  Publication Details (including relevant citation   information):

  Schaff and Montgomery

  "An HPLC-HR-MSMS Method for Identification of Anticoagulant   Rodenticides in Blood

  Journal of Analytical Toxicology, v 37, pp 321-325, 2013.


  This paper presents a fully validated method for the qualitative   identification of bromadiolone, brodifacoum, coumachlor,   coumatetralyl, difenacoum and warfarin in whole blood specimens.   Samples are protein precipitated with acetonitrile, processed via   solid-phase extraction and analyzed by high-performance liquid   chromatography with high resolution tandem mass spectrometric   detection. Limits of detection were 10 ng/mL or better for all   analytes.

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