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GC FID acetic acid assay test

Dear colleagues,

Does anyone that have experience dealing with acetic acid glacial assay determination using GC with FID can share any word of advice?.  The ACS Regent Chemical monograph points out Chromatographic procedure to solve this, but searching on it there is no specific procedure to follow for achieving such assay determination.  I'm particularly interested on any existing procedure about how to prepare the standard solutions.


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