Brought to you by:
Speakers:
Dr. Brian Rodenhausen
Particle and Materials Characterization Lead Scientist,
Anton Paar
Dr. Abhishek Shetty
Advanced Technical Center Lead Scientist,
Anton Paar
Kelly McSweeney
Contributing Editor,
C&EN Media Group
When developing and producing food products, it is essential to do in-depth powder analysis to guarantee the highest standards of quality, safety, and uniformity. Powdered foods can be adequately characterised using a wide range of analytical techniques. Key analytical methods typically employed for characterising food powders include:
**Particle Size Analysis**: The flowability, solubility, and texture of a food powder are all significantly impacted by the particle size distribution. Particle size distribution and average particle size can be measured with tools including laser diffraction, sedimentation, and microscopy.
Scanning electron microscopy (SEM) produces high-resolution images of the surfaces of food powders, revealing the morphology, size, and shape of individual particles. Knowing how particles interact and pack together is greatly aided by this data.
X-ray diffraction (XRD) is a method for determining the presence of crystalline structures in powdered foods. The purity and stability of ingredients, as well as how they could react with one another during manufacturing and storage, can be evaluated in this way.
Fourier transform infrared spectroscopy (FTIR) measures the infrared absorption spectra of food powders to determine their molecular makeup. It can classify functional groups, which is useful for characterising ingredients and keeping tabs on processing-related shifts.
Using a device called a **differential scanning calorimeter** (DSC), scientists may determine the rate of heat transfer in a powdered food item at varying temperatures. Phase changes, melting points, and thermal stability are all things that can be investigated with this method.
Moisture analysis is an important factor in determining the freshness and longevity of food powder. Karl Fischer titration, loss on drying, and near-infrared spectroscopy are all useful techniques for determining moisture content.
7. **Density Measurements in Bulk and on the Taps**: Powders' packing and flow behaviour can be better understood with the use of these metrics. While tap density takes into account the packing after tapping, bulk density measures the mass of powder per unit volume.
Rheological analysis, number eight, looks at how food powders deform and flow when pressure is applied. Powder behaviour during processing can be better understood by rheological measures, which can then be used to inform the creation of goods like doughs and batters.
Colour is an important sensory attribute of food powders, and it can be evaluated here. Colorimeters and spectrophotometers help with quality control and guarantee a uniform look by measuring and reporting on colour properties including hue, brightness, and saturation.
The flowability of a powder can be measured in a number of ways, including the flowability index and the angle of repose. For efficient processing and packaging, this data is crucial.
Brunauer-Emmett-Teller (BET) analysis can be used to calculate the specific surface area of powders; this information is useful for elucidating their reactivity, adsorption, and dissolution kinetics.
Dynamic light scattering (DLS) is a technique for determining the size of suspended particles by analysing their ability to scatter light. Some food powders contain nanoparticles or emulsions, and this method can help you learn more about them.
When making the leap from research and development to manufacturing, it's crucial that the analytic methods employed are suitable for use in industrial settings. It may be necessary to modify some processes in order to keep up with the increased volume and velocity of manufacturing without sacrificing accuracy or precision. The choice of methods will also be affected by the requirements of the product and the process.